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La ricerca find articoli where soggetti phrase all words 'GAMMA-BUTYROLACTONES' sort by level,fasc_key/DESCEND, pagina_ini_num/ASCEND ha restituito 231 riferimenti
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    1. Steurer, S; Podlech, J
      Indium-catalyzed Barbier reactions of amino aldehydes

      ADVANCED SYNTHESIS & CATALYSIS
    2. Bohm, C; Reiser, O
      Enantioselective synthesis of (-)-roccellaric acid

      ORGANIC LETTERS
    3. Enholm, EJ; Cottone, JS
      Highly diastereoselective radical cyclizations on soluble ring opening metathesis supports

      ORGANIC LETTERS
    4. Nacro, K; Gorrichon, L; Escudier, JM; Baltas, M
      Stereochemistry control in the Lewis acid mediated lactonization reaction of gamma,delta-epoxy-beta-silyloxy esters

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    5. Miyabe, H; Fujii, K; Tanaka, H; Naito, T
      Solid-phase tandem radical addition-cyclisation reaction of oxime ethers

      CHEMICAL COMMUNICATIONS
    6. Lawrence, NJ; McGown, AT; Nduka, J; Hadfield, JA; Pritchard, RG
      Cytotoxic Michael-type amine adducts of alpha-methylene lactones alantolactone and isoalantolactone

      BIOORGANIC & MEDICINAL CHEMISTRY LETTERS
    7. Benedetti, F; Forzato, C; Nitti, P; Pitacco, G; Valentin, E; Vicario, M
      Synthesis of all stereoisomers of cognac lactones via microbial reduction and enzymatic resolution strategies

      TETRAHEDRON-ASYMMETRY
    8. Brenna, E; Dei Negri, C; Fuganti, C; Serra, S
      Baker's yeast-mediated approach to (-)-cis- and (+)-trans-Aerangis lactones

      TETRAHEDRON-ASYMMETRY
    9. Kongsaeree, P; Meepowpan, P; Thebtaranonth, Y
      Synthesis of both enantiomers of methylenolactocin, nephrosterinic acid and protolichesterinic acid via tandem aldol-lactonization reactions

      TETRAHEDRON-ASYMMETRY
    10. Roy, SC; Guin, C; Rana, KK; Maiti, G
      Ceric ammonium nitrate mediated selective bromoalkoxylation of activated cinnamyl compounds using lithium bromide

      SYNLETT
    11. Ariza, X; Garcia, J; Lopez, M; Montserrat, L
      A concise synthesis of (-)-methylenolactocin and (-)- phaseolinic acid from (6S,9S)-tetradec-7-yne-6,9-diol

      SYNLETT
    12. Fazio, F; Maliakal, D; Schneider, MP
      Convenient new syntheses of R-(+)-5-Benzyloxymethyl-5H-furan-2-one- a building block en route to L-nucleosides

      HETEROCYCLES
    13. Fukuzawa, S; Miura, M; Matsuzawa, H
      Diastereoselective reduction and carbon-carbon bond formation of alpha-keto esters/amides with SmI2

      TETRAHEDRON LETTERS
    14. Loh, TP; Lye, PL
      A concise synthesis of (+/-)-methylenolactocin and the formal synthesis of(+/-)-phaseolinic acid

      TETRAHEDRON LETTERS
    15. Janecki, T; Blaszczyk, E
      Stereocontrolled synthesis of 5-(1 '-hydroxyalkyl)-3-methylidenetetrahydro-2-furanones

      TETRAHEDRON LETTERS
    16. Bella, M; Piancatelli, G; Squarcia, A
      Efficient preparation of 3-substituted-furan-2(5H)-ones and their direct vinylogous aldol addition

      TETRAHEDRON
    17. Gossinger, E; Schwartz, A; Sereinig, N
      Approach towards an EPC synthesis of nodusmicin. Part 5: Stereoselective introduction of a side chain at the cis-decalin part of nodusmicin

      TETRAHEDRON
    18. Srikrishna, A; Danieldoss, S
      Radical cyclisation based approach to lignans. Synthesis of 4-arylmethyldihydrofuran-2-ones

      SYNTHETIC COMMUNICATIONS
    19. Silva, LF
      Total synthesis of bakkanes

      SYNTHESIS-STUTTGART
    20. Janecki, T; Blaszczyk, E
      A convenient synthesis of 3-alkylidenetetrahydro-2-furanones from 3-diethoxyphosphoryl-2,5-dihydro-2-furanones

      SYNTHESIS-STUTTGART
    21. Patra, A; Batra, S; Kundu, B; Joshi, BS; Roy, R; Bhaduri, AP
      5-isoxazolecarboxaldehyde: A novel substrate for fast Baylis-Hillman reaction

      SYNTHESIS-STUTTGART
    22. Ballini, R; Bosica, G; Livi, D
      A new synthesis of exo-methylene butyrolactones from nitroalkanes

      SYNTHESIS-STUTTGART
    23. Zhang, QH; Lu, XY; Han, XL
      Palladium(II)-catalyzed asymmetric cyclization of (Z)-4 '-acetoxy-2 '-butenyl 2-alkynoates. Role of nitrogen-containing ligands in palladium(II)-mediated reactions

      JOURNAL OF ORGANIC CHEMISTRY
    24. Cossy, J; Rasamison, C; Pardo, DG
      Reactivity of alpha-(benzoyloxy)crotylstannane with aldehydes in liquid phase and on solid support. Synthesis of substituted lactones

      JOURNAL OF ORGANIC CHEMISTRY
    25. Paleta, O; Palecek, J; Dolensky, B
      Fluorinated butanolides and butenolides Part 8. 2-(trifluoromethyl)butan-4-olides by synthesis from methyl 3,3,3-trifluoropyruvate as building block

      JOURNAL OF FLUORINE CHEMISTRY
    26. Takeuchi, S; Ukaji, Y; Inomata, K
      Asymmetric bis(alkoxycarbonylation) reaction of terminal olefins catalyzedby palladium in the presence of copper(I) triflate and a chiral bioxazoline ligand

      BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
    27. Yorimitsu, H; Shinokubo, H; Oshima, K
      Radical reaction by a combination of phosphinic acid and a base in aqueousmedia

      BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
    28. Villar, F; Equey, O; Renaud, P
      Desymmetrization of 1,4-dien-3-ols and related compounds via Ueno-Stork radical cyclizations

      ORGANIC LETTERS
    29. Ward, DE; Gai, YZ; Qiao, Q
      A general approach to cyathin diterpenes. Total synthesis of allocyathin B-3

      ORGANIC LETTERS
    30. Drioli, S; Felluga, F; Forzato, C; Pitacco, G; Valentin, E
      Synthesis and biological resolution of condensed bicyclic isoparaconic acid derivatives

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    31. Jabre-Truffert, S; Delmas, AM; Grennberg, H; Akermark, B; Waegell, B
      Evidence for the intermediacy of (eta(3)-allyl)palladium complexes in the palladium-catalyzed acryloxylation of cycloalkenes: Unexpected oxidation of1,5-cyclooctadiene

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    32. Krawczyk, E; Skowronska, A
      A novel one-pot synthetic method for alpha-methylenation of lactones and cycloalkanones based on thiophosphates

      HETEROATOM CHEMISTRY
    33. Drioli, S; Forzato, C; Nitti, P; Pitacco, G; Valentin, E
      Chemoenzymatic synthesis of optically active 4-methyl-tetrahydro-5-oxo-2-furancarboxylic acids and esters

      TETRAHEDRON-ASYMMETRY
    34. Missio, LJ; Comasseto, JV
      Enantioselective synthesis of (-)-gamma-jasmolactone

      TETRAHEDRON-ASYMMETRY
    35. El Ali, B; Alper, H
      The application of transition metal catalysis for selective cyclocarbonylation reactions. Synthesis of lactones and lactams

      SYNLETT
    36. Tzeng, CC; Lee, KH; Wang, TC; Han, CH; Chen, YL
      Synthesis and cytotoxic evaluation of a series of gamma-substituted gamma-aryloxymethyl-alpha-methylene-gamma-butyrolactones against cancer cells

      PHARMACEUTICAL RESEARCH
    37. Hassan, HHAM
      Synthesis of bridged head methyl 3,4-O-(1 ',2 '-dimethylcycloheaxane-1 ',2'-diyl)-6,7-dideoxy-alpha-D-mannooct-6-enepyranose-8,2-lactone from D-mannose

      HETEROCYCLES
    38. Pastor, IM; Yus, M
      Lithium- alpha-lithioacetate and beta-lithiopropionate: useful intermediates in organic synthesis

      TETRAHEDRON LETTERS
    39. Kiegiel, J; Nowacki, J; Tarnowska, A; Stachurska, M; Jurczak, J
      A new asymmetric route to synthetically useful gamma-substituted gamma-butyrolactones

      TETRAHEDRON LETTERS
    40. Gaudin, JM
      Synthesis and organoleptic properties of p-menthane lactones

      TETRAHEDRON
    41. Lin, P; Jiang, JL
      Synthesis of monotrifluoromethyl-substituted saturated cycles

      TETRAHEDRON
    42. Cao, WG; Ding, WY; Chen, YL; Gao, JS
      An efficient and highly stereoselective synthesis of cis-1-acetyl-2-aryl-6,6-dimethyl-5,7-dioxo-spiro-[2,5]-4,8-octadiones and beta,gamma-trans-beta-acetyl-gamma-aryl-butyrolactones

      SYNTHETIC COMMUNICATIONS
    43. Cao, WG; Ding, WY; Chen, YL; Gao, JS
      Study on the reaction of cis-1-acetyl-2-aryl-6,6-dimethyl-5,7-dioxo-spiro-[2,5]-4,8-octadiones with methanol

      SYNTHETIC COMMUNICATIONS
    44. Ha, HJ; Lee, SY; Park, YS
      Stereocontrolled iodolactonization of acyclic olefinic amides

      SYNTHETIC COMMUNICATIONS
    45. Steinbach, JH; Bracamontes, J; Yu, L; Zhang, PN; Covey, DF
      Subunit-specific action of an anticonvulsant thiobutyrolactone on recombinant glycine receptors involves a residue in the M2 membrane-spanning region

      MOLECULAR PHARMACOLOGY
    46. Michaut, M; Santelli, M; Parrain, JL
      Efficient synthesis of spirolactones from cyclic anhydrides via an allylation/alkylation-RCM sequence

      JOURNAL OF ORGANOMETALLIC CHEMISTRY
    47. Somech, I; Shvo, Y
      Synthesis of gamma-lactones and unsaturated bis gamma-lactones via Cu-Fe-mediated reductive cyclization of di- and tri-alpha-halogenated carboxylic esters

      JOURNAL OF ORGANOMETALLIC CHEMISTRY
    48. Seki, M; Shimizu, T; Matsumoto, K
      Stereoselective synthesis of beta-benzyl-alpha-alkyl-beta-amino acids fromL-aspartic acid

      JOURNAL OF ORGANIC CHEMISTRY
    49. Kamitani, A; Chatani, N; Morimoto, T; Murai, S
      Carbonylative [5+1] cycloaddition of cyclopropyl imines catalyzed by ruthenium carbonyl complex

      JOURNAL OF ORGANIC CHEMISTRY
    50. Chen, MJ; Lo, CY; Chin, CC; Liu, RS
      Total synthesis of (+)-blastmycinone, (-)-litsenolide C-1, and related natural trisubstituted lactones via alkynyltungsten compounds

      JOURNAL OF ORGANIC CHEMISTRY
    51. Fang, KC; Chen, YL; Sheu, JY; Wang, TC; Tzeng, CC
      Synthesis, antibacterial, and cytotoxic evaluation of certain 7-substituted norfloxacin derivatives

      JOURNAL OF MEDICINAL CHEMISTRY
    52. Paleta, O; Volkov, A; Hetflejs, J
      Fluorinated butanolides and butenolides. Part 5. Synthesis and nucleophilic reactions of 3-chloro-2-fluoro-2-buten-4-olide as tetronic acid analogue.Conjugate addition of hard nucleophiles and vinylic halogen displacement with soft phosphorus nucleophiles

      JOURNAL OF FLUORINE CHEMISTRY
    53. Kvicala, J; Vlasakova, R; Plocar, J; Paleta, O; Pelter, A
      Preparation of intermediates for fluorinated lignans by conjugated and tandem additions on 3-fluorofuran-2(5H)-one

      COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS
    54. Eliel, EL; Bai, X; Ohwa, M
      Enantioselective syntheses of substituted gamma-butyrolactones

      JOURNAL OF THE CHINESE CHEMICAL SOCIETY
    55. Chen, IL; Wang, TC; Chen, YL; Tzeng, CC
      Aluminium chloride-catalyzed intermolecular vs intramolecular Friedel-Crafts reaction of acrylanilides and 3-chloropropanamides

      JOURNAL OF THE CHINESE CHEMICAL SOCIETY
    56. Chinchilla, R; Najera, C
      Acylvinyl and vinylogous synthons

      CHEMICAL REVIEWS
    57. Okamoto, S; Livinghouse, T
      Titanium(IV) aryloxide catalyzed cyclization reactions of 1,6-and 1,7-dienes

      JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
    58. Yorimitsu, H; Nakamura, T; Shinokubo, H; Oshima, K; Omoto, K; Fujimoto, H
      Powerful solvent effect of water in radical reaction: Triethylborane-induced atom-transfer radical cyclization in water

      JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
    59. Bissel, P; Nazih, A; Sablong, R; Lepoittevin, JP
      Stereoselective synthesis of (R)- and (S)-4-methoxydalbergione via asymmetric catalytic hydrogenation

      ORGANIC LETTERS
    60. Blandin, V; Carpentier, JF; Mortreux, A
      Asymmetric hydrogenation of 2,4-dioxo esters: Selective synthesis of 2-hydroxy-4-oxo esters and direct access to chiral 2-hydroxy-4-butyrolactones

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    61. Steurer, S; Podlech, J
      Aminoalkyl-substituted alpha-methylene-gamma-butyrolactones from alpha-amino acids using an indium-mediated Barbier allyl addition

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    62. Arcadi, A; Cacchi, S; Fabrizi, G; Moro, L
      Palladium-catalyzed cyclocarbonylation of o-ethynylphenols and vinyl triflates to form 3-alkylidene-2-coumaranones

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    63. Ramachandran, PV; Krzeminski, MP; Reddy, MVR; Brown, HC
      A facile synthesis of chiral omega-allyl- and omega-n-propyllactones via asymmetric allylboration of formyl esters with B-allyldiisopinocampheylborane

      TETRAHEDRON-ASYMMETRY
    64. Hill, MW; de la Cruz, MAM; Covey, DF; Rothman, SM
      Effects of anticonvulsant lactams on in vitro seizures in the hippocampal slice preparation

      EPILEPSY RESEARCH
    65. Tada, M
      Reactions of alkyl-cobalt complexes

      REVIEWS ON HETEROATOM CHEMISTRY
    66. Csuk, R; Schroder, C
      Allylphosphonates by heteroanalogous zinc-silver/graphite mediated Dreiding-Schmidt reactions

      JOURNAL OF CARBOHYDRATE CHEMISTRY
    67. de March, P; Figueredo, M; Font, J
      1,3-dipolar cycloadditions of five and six membered cyclic nitrones to alpha,beta-unsaturated acid derivatives

      HETEROCYCLES
    68. Lubineau, A; Auge, J
      Water as solvent in organic synthesis

      MODERN SOLVENTS IN ORGANIC SYNTHESIS
    69. Nagano, H; Ohtani, Y; Odake, E; Nakagawa, J; Mori, Y; Yajima, T
      Tandem 5-exo-dig-5-exo-trig radical cyclization leading to a 6,5-ring fused carbobicycle possessing two contiguous quaternary carbons at the bridgehead and its adjacent positions

      JOURNAL OF CHEMICAL RESEARCH-S
    70. Lim, J; Kim, YH
      Stereoselective synthesis of 1 'beta-2 ',3 '-dideoxy-2 '-bis(ethoxycarbonyl)methyluridine nucleosides by ring opening of cyclopropanated glycals

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    71. Thomas, EJ; Watts, JP
      Synthesis of cytochalasans using intramolecular Diels-Alder reactions: an alternative approach to cytochalasin D

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    72. Srikrishna, A; Nagaraju, S; Venkateswarlu, S; Hiremath, US; Reddy, TJ; Venugopalan, P
      A formal total synthesis of (+/-)-homogynolide-B

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    73. Voelter, W; Thurmer, R; Al-Qawasmeh, RA; Al-Tel, TH; Abdel-Jalil, R; Al-Abed, Y
      Epoxy pyranoses, chiral synthons for versatile regio- and stereocontrolledfunctionalizations

      POLISH JOURNAL OF CHEMISTRY
    74. Hashem, A; Senning, A
      Reactions of 2(3H)-furanones

      ADVANCES IN HETEROCYCLIC CHEMISTRY, VOL 73
    75. Fotiadu, F; Pardigon, O; Buono, G; Le Corre, M; Hercouet, A
      Efficient synthesis of 3-methylene-2-pyrrolidinone and highly exoselectiveDiels-Alder addition to cyclopentadiene

      TETRAHEDRON LETTERS
    76. Madec, D; Henryon, V; Ferezou, JP
      Easy transformations of vinyl N,N-diisopropyl carbamates into silyl enol ethers or aldehydes by addition of methyllithium

      TETRAHEDRON LETTERS
    77. Kise, N; Hirata, Y; Hamaguchi, T; Ueda, N
      Stereoselective coupling of optically active 3-trans-cinnamoyl-2-oxazolidinones with acid anhydrides by electroreduction

      TETRAHEDRON LETTERS
    78. Silveira, CC; Bernardi, CR; Braga, AL; Kaufman, TS
      Pictet-Spengler condensation of N-sulfonyl-beta-phenethylamines with alpha-chloro-alpha-phenylselenoesters. New synthesis of 1,2,3,4-tetrahydroisoquinoline-1-carboxylates

      TETRAHEDRON LETTERS
    79. Villar, F; Andrey, O; Renaud, P
      Diastereoselective radical cyclization of bromoacetals: Efficient synthesis of (+/-)-botryodiplodin

      TETRAHEDRON LETTERS
    80. Harrowven, DC; Lucas, MC; Howes, PD
      A simple and direct method for converting thioamides into thioesters

      TETRAHEDRON
    81. Li, CJ; Chan, TH
      Organic syntheses using indium-mediated and catalyzed reactions in aqueousmedia

      TETRAHEDRON
    82. Mandal, PK; Roy, SC
      Total synthesis of (+/-)-dihydroprotolichesterinic acid and formal synthesis of (+/-)-roccellaric acid by radical cyclisation of an epoxide using a transition-metal radical source

      TETRAHEDRON
    83. Cacchi, S
      Heterocycles via cyclization of alkynes promoted by organopalladium complexes

      JOURNAL OF ORGANOMETALLIC CHEMISTRY
    84. Kocovsky, P; Ahmed, G; Srogl, J; Malkov, AV; Steele, J
      New Lewis-acidic molybdenum(II) and tungsten(II) catalysts for intramolecular carbonyl ene and prins reactions. Reversal of the stereoselectivity of cyclization of citronellal

      JOURNAL OF ORGANIC CHEMISTRY
    85. Peterson, MA; Nilsson, BL; Sarker, S; Doboszewski, B; Zhang, WJ; Robins, MJ
      Amide-linked ribonucleoside dimers derived from 5 '-amino-5 '-deoxy- and 3'-(carboxymethyl)-3 '-deoxynucleoside precursors

      JOURNAL OF ORGANIC CHEMISTRY
    86. Gabriele, B; Salerno, G; De Pascali, F; Costa, M; Chiusoli, GP
      An efficient and general synthesis of furan-2-acetic esters by palladium-catalyzed oxidative carbonylation of (Z)-2-en-4-yn-1-ols

      JOURNAL OF ORGANIC CHEMISTRY
    87. Shiu, LH; Li, YL; Li, CL; Lao, CY; Chen, WC; Yu, CH; Liu, RS
      Stereocontrolled synthesis of functionalized bicyclic cx-methylene butyrolactones via tungsten-mediated intramolecular allylation of aldehydes

      JOURNAL OF ORGANIC CHEMISTRY
    88. Li, JH; Jiang, HF; Feng, AQ; Jia, LQ
      Novel stereospecific synthesis of 3-chloroacrylate esters via palladium-catalyzed carbonylation of terminal acetylenes

      JOURNAL OF ORGANIC CHEMISTRY
    89. Ramachandran, PV; Reddy, MVR; Brown, HC
      An efficient enantioselective synthesis of argentilactone

      JOURNAL OF THE INDIAN CHEMICAL SOCIETY
    90. Sibi, MP
      Are two phenyls better than one? Synthesis and applications of (R)-4-diphenylmethyl-2-oxazolidinone

      ALDRICHIMICA ACTA
    91. HAMPEL F; HOMMES NV; HOOPS S; MAAREF F; SCHOBERT R
      NOVEL 9-MEMBERED TITANAHETEROCYCLES - STRUCTURE, AB-INITIO CALCULATIONS, AND PREPARATIVE USE TOWARDS THE SELECTIVE SYNTHESIS OF SUBSTITUTEDCYCLOPENTANOLS

      EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
    92. SCHABBERT S; SCHAUMANN E
      PALLADIUM-CATALYZED CYCLIZATION OF SILYL-SUBSTITUTED BIS(HOMO)PROPARGYLIC ALCOHOLS TO 2,3-DIHYDROFURANS

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    93. FRAGALE G; WIRTH T
      CHIRAL DISELENIDES IN ASYMMETRIC CYCLIZATION REACTIONS

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    94. CANNEY DJ; LU HF; MCKEON AC; YOON KW; XU K; HOLLAND KD; ROTHMAN SM; FERRENDELLI JA; COVEY DF
      STRUCTURE-ACTIVITY STUDIES OF FLUOROALKYL-SUBSTITUTED GAMMA-BUTYROLACTONE AND GAMMA-THIOBUTYROLACTONE MODULATORS OF GABA(A) RECEPTOR FUNCTION

      Bioorganic & medicinal chemistry
    95. NISHIKORI H; ITO K; KATSUKI T
      A SHORT-STEP SYNTHESIS OF TRANS-WHISKEY LACTONE BY AN ASYMMETRIC MICHAEL REACTION

      Tetrahedron : asymmetry
    96. FURSTNER A
      MULTICOMPONENT CATALYSIS FOR REDUCTIVE BOND FORMATIONS

      Chemistry
    97. ENDERS D; DYKER H; LEUSINK FR
      ENANTIOSELECTIVE SYNTHESIS OF PROTECTED ISOTETRONIC ACIDS

      Chemistry
    98. HARCKEN C; BRUCKNER R; RANK E
      TOTAL SYNTHESES OF (-)-GRANDINOLIDE AND (-)-SAPRANTHIN BY THE SHARPLESS ASYMMETRIC DIHYDROXYLATION OF METHYL TRANS-3-PENTENOATE - ELUCIDATION OF THE STEREOSTRUCTURE OF (-)-SAPRANTHIN

      Chemistry (Weinheim)
    99. SHIMIZU M; KAMIKUBO T; OGASAWARA K
      AN ENANTIOCONTROLLED AND DIASTEREOCONTROLLED ROUTE TO MINTLACTONE ANDISOMINTLACTONE USING A CHIRAL CYCLOHEXADIENONE EQUIVALENT

      Synlett
    100. LU XY; ZHU GX; WANG Z
      ENYNE COUPLING AS THE POTENT METHODOLOGY FOR THE SYNTHESIS OF BIOACTIVE MOLECULES

      Synlett


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Documento generato il 17/01/21 alle ore 22:45:46