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    1. Lammerhofer, M; Zarbl, E; Piette, V; Crommen, J; Lindner, W
      Evaluation of enantioselective nonaqueous ion-pair capillary electrophoresis as screening assay in the development of new ion exchange type chiral stationary phases

      JOURNAL OF SEPARATION SCIENCE
    2. Ashton, PR; Harris, KDM; Kariuki, BM; Philp, D; Robinson, JMA; Spencer, N
      A borazaaromatic analogue of isophthalic acid

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2
    3. Aggarwal, VK; Angelaud, R; Bihan, D; Blackburn, P; Fieldhouse, R; Fonquerna, SJ; Ford, GD; Hynd, G; Jones, E; Jones, RVH; Jubault, P; Palmer, MJ; Ratcliffe, PD; Adams, H
      Synthesis and evaluation of a broad range of chiral sulfides for asymmetric sulfur ylide epoxidation of aldehydes

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    4. Iuliano, A; Attolino, E; Salvadori, P
      (S)-leucine and [(S)-1-(1-naphthyl)ethyl]amine as chiral building blocks for a bifunctional system - Synthesis of a new chiral stationary phase and evaluation of its biselector properties in the HPLC resolution of racemic compounds

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    5. Brown, RCD; Keily, JF
      Asymmetric permanganate-promoted oxidative cyclization of 1,5-dienes by using chiral phase-transfer catalysis

      ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
    6. Spivey, AC; Andrews, BI
      Catalysis of the asymmetric desymmetrization of cyclic anhydrides by nucleophilic ring-opening with alcohols

      ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
    7. Belokon, YN; Kochetkov, KA; Churkina, TD; Ikonnikov, NS; Larionov, OV; Harutyunyan, SR; Vyskocil, S; North, M; Kagan, HB
      Highly efficient catalytic synthesis of alpha-amino acids under phase-transfer conditions with a novel catalyst/substrate pair

      ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
    8. Huc, I; Nguyen, R
      Dynamic combinatorial chemistry

      COMBINATORIAL CHEMISTRY & HIGH THROUGHPUT SCREENING
    9. Silva, THA; Oliveira, AB; Dos Santos, HF; De Almeida, WB
      Conformational analysis of epiquinine and epiquinidine

      STRUCTURAL CHEMISTRY
    10. Pytel, P; Oleksyn, BJ; Sliwinski, J
      Crystal and molecular structure of a new cobalt complex of quinine

      ENANTIOMER
    11. Zhang, J; Wu, XY; Zhou, QL; Sun, J
      Chiral camphor derivatives as new catalysts for asymmetric phase-transfer alkylation

      CHINESE JOURNAL OF CHEMISTRY
    12. O'Donnell, MJ; Delgado, F; Dominguez, E; de Blas, J; Scott, WL
      Enantioselective solution- and solid-phase synthesis of glutamic acid derivatives via Michael addition reactions

      TETRAHEDRON-ASYMMETRY
    13. Dai, WM; Yeung, KKY; Chow, CW; Williams, ID
      Study on enantiomerically pure 2-substituted N,N-dialkyl-1-naphthamides: resolution, absolute stereochemistry, and application to desymmetrization ofcyclic meso anhydrides

      TETRAHEDRON-ASYMMETRY
    14. Gawronski, J; Gawronska, K; Kacprzak, K
      Chiral C and S conformers of aromatic diimide triads

      CHIRALITY
    15. Szollosi, G; Bartok, M
      Enantioselective Michael addition catalyzed by cinchona alkaloids

      CHIRALITY
    16. Szollosi, G; Kun, I; Bartok, M
      Heterogeneous asymmetric reactions. Part 24. Heterogeneous catalytic enantioselective hydrogenation of the C=N group over cinchona alkaloid modified palladium catalyst

      CHIRALITY
    17. Itoh, T; Shirakami, S
      Synthesis of chiral azacrown ethers derived from alpha-D-glucose and theircatalytic properties on the asymmetric Michael addition

      HETEROCYCLES
    18. Greig, LM; Philp, D
      Applying biological principles to the assembly and selection of synthetic superstructures

      CHEMICAL SOCIETY REVIEWS
    19. Lygo, B; To, DCM
      Improved procedure for the room temperature asymmetric phase-transfer mediated epoxidation of alpha,beta-unsaturated ketones

      TETRAHEDRON LETTERS
    20. Kim, DY; Huh, SC; Kim, SM
      Enantioselective Michael reaction of malonates and chalcones by phase-transfer catalysis using chiral quaternary ammonium salt

      TETRAHEDRON LETTERS
    21. Uozumi, Y; Yasoshima, K; Miyachi, T; Nagai, S
      Enantioselective desymmetrization of meso-cyclic anhydrides catalyzed by hexahydro-1H-pyrrolo[1,2-c] imidazolones

      TETRAHEDRON LETTERS
    22. Houjou, H; Nagawa, Y; Hiratani, K
      Spontaneous macrocyclization via recombination of a Schiff-base linkage

      TETRAHEDRON LETTERS
    23. Kim, DY; Huh, SC
      Enantioselective Michael reaction of nitroalkanes and chalcones by phase-transfer catalysis using chiral quaternary ammonium salts

      TETRAHEDRON
    24. Lygo, B; Crosby, J; Lowdon, TR; Peterson, JA; Wainwright, PG
      Studies on the enantioselective synthesis of alpha-amino acids via asymmetric phase-transfer catalysis

      TETRAHEDRON
    25. Kacprzak, K; Gawronski, J
      Cinchona alkaloids and their derivatives: Versatile catalysts and ligands in asymmetric synthesis

      SYNTHESIS-STUTTGART
    26. Bolm, C; Schiffers, I; Dinter, CL; Defrere, L; Gerlach, A; Raabe, G
      Efficient asymmetric synthesis of unnatural beta-amino acids

      SYNTHESIS-STUTTGART
    27. Choi, CH; Tian, SK; Deng, L
      A formal catalytic asymmetric synthesis of (+)-biotin with modified cinchona alkaloids

      SYNTHESIS-STUTTGART
    28. Thiel, J; Katrusiak, A; Fiedorow, P
      Cinchona alkaloids: the structure of beta-isocinchonicine revisited

      JOURNAL OF MOLECULAR STRUCTURE
    29. Vargas, A; Burgi, T; Baiker, A
      Model of reactant-modifier interaction in enantioselective hydrogenation of ethyl pyruvate on platinum-cinchona catalysts: Extension to synthetic chiral modifiers

      JOURNAL OF CATALYSIS
    30. Marchais, S; Vermeulen, ES; Semple, G; Sundell, S; Wikstrom, HV
      Ion-pair formation of hydroquinine by chromatography

      ANALYTICA CHIMICA ACTA
    31. Stork, G; Niu, D; Fujimoto, A; Koft, ER; Balkovec, JM; Tata, JR; Dake, GR
      The first stereoselective total synthesis of quinine

      JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
    32. Bartok, T; Felfoldi, K; Szollosi, G; Bartok, M; Dega-Szafran, Z; Thiel, J
      Mass spectra of iso-cinchona- and halogenated cinchona alkaloids

      EUROPEAN JOURNAL OF MASS SPECTROMETRY
    33. Brunner, H; Schmidt, P
      Asymmetric catalysis, 131 - Naproxen derivatives by enantioselective decarboxylation

      EUROPEAN JOURNAL OF ORGANIC CHEMISTRY
    34. Langer, P
      New strategies for the development of an asymmetric version of the Baylis-Hillman reaction

      ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
    35. Handy, ST
      Asymmetric catalysis: A ligand's eye view

      CURRENT ORGANIC CHEMISTRY
    36. Danieli, B; Lesma, G; Passarella, D; Silvani, A
      A chemo-enzymatic approach to some indole and quinolizidine alkaloids fromC-s-symmetric precursors

      CURRENT ORGANIC CHEMISTRY
    37. Song, CE; Lim, JS; Kim, SC; Lee, KJ; Chi, DY
      Immobilisation of ketone catalyst: a method to prevent ketone catalyst from decomposing during dioxirane-mediated epoxidation of alkenes

      CHEMICAL COMMUNICATIONS
    38. Bartok, T; Szollosi, G; Felfoldi, K; Bartok, M; Thiel, J
      New results on the mass spectra of cinchona alkaloids

      JOURNAL OF MASS SPECTROMETRY
    39. Brunner, H; Schmidt, P; Prommesberger, M
      Enantioselective catalysis. Part 133: Conformational analysis of amides of9-amino(9-deoxy)epicinchonine

      TETRAHEDRON-ASYMMETRY
    40. Mroczek, T; Glowniak, K
      TLC and HPTLC assay of quinoline and quinuclidine alkaloids in Cinchonae cortex and pharmaceutical preparations

      JPC-JOURNAL OF PLANAR CHROMATOGRAPHY-MODERN TLC
    41. Brunner, H; Schmidt, P
      Asymmetric catalysis, 134. Naproxen derivatives by enantioselective decarboxylation

      ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES
    42. Kubicki, M; Borowiak, T; Gawronska, K; Gawronski, J
      Formation and structure of cinchona alkaloid (bis-2,3-naphthalenediyl)orthoborate salts

      ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES
    43. Schefzick, S; Lindner, W; Lipkowitz, KB; Jalaie, M
      Enantiodiscrimination by a quinine-based chiral stationary phase: A computational study

      CHIRALITY
    44. Sakai, T
      Role of cinchona-alkaloids on the formation of ion associates between sulphonephthalein dyestuffs and quaternary ammonium ions

      BUNSEKI KAGAKU
    45. Ferri, D; Burgi, T; Baiker, A
      Conformational isomerism of a-ketoesters. A FTIR and ab initio study

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2
    46. Hubel, R; Polborn, K; Knizek, J; Noth, H; Beck, W
      Metal complexes of biologically important ligands. CXXVI. Palladium(II) and platinum(II) complexes with the antimalarial drug mefloquine as ligand

      ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
    47. Belokon', YN; Davies, RG; North, M
      A practical asymmetric synthesis of alpha-methyl alpha-amino acids using achiral Cu-salen complex as a phase transfer catalyst

      TETRAHEDRON LETTERS
    48. O'Neil, IA; Wynn, D; Lai, JYQ
      The synthesis and functionalisation of quinuclidine enamine N-oxide and borane complex

      TETRAHEDRON LETTERS
    49. Belokon, YN; Kochetkov, KA; Churkina, TD; Ikonnikov, NS; Chesnokov, AA; Larionov, OV; Singh, I; Parmar, VS; Vyskocil, S; Kagan, HB
      Asymmetric PTC C-alkylation catalyzed by chiral derivatives of tartaric acid and aminophenols. Synthesis of (R)- and (S)-alpha-methyl amino acids

      JOURNAL OF ORGANIC CHEMISTRY
    50. Niwayama, S
      Highly efficient selective monohydrolysis of symmetric diesters

      JOURNAL OF ORGANIC CHEMISTRY
    51. Frackenpohl, J; Hoffmann, HMR
      Synthesis of enantiopure 3-quinuclidinone analogues with three stereogeniccenters: (1S,2R,4S)- and (1S,2S,4S)-2-(hydroxymethyl)-1-azabicyclo[2.2.2]octan-5-one and stereocontrol of nucleophilic addition to the carbonyl group

      JOURNAL OF ORGANIC CHEMISTRY
    52. Uccello-Barretta, G; Balzano, F; Quintavalli, C; Salvadori, P
      Different enantioselective interaction pathways induced by derivatized quinines

      JOURNAL OF ORGANIC CHEMISTRY
    53. Roy, BN; Kumar, A; Sankaran, R
      Emerging trends in synthesis of drugs and fine chemicals

      JOURNAL OF THE INDIAN CHEMICAL SOCIETY
    54. Franco, P; Lammerhofer, M; Klaus, PM; Lindner, W
      Novel cinchona alkaloid O-9-hydrazide derivatives as chiral anion-exchange-type selectors: Synthesis and chromatographic evaluation

      CHROMATOGRAPHIA
    55. Schrake, O; Rahn, VS; Frackenpohl, J; Braje, WM; Hoffmann, HMR
      Novel bridged bicyclic alpha-amino acid eaters and key derivatives from quincorine and quincoridine

      ORGANIC LETTERS
    56. Nelson, A
      Asymmetric phase-transfer catalysis

      ANGEWANDTE CHEMIE-INTERNATIONAL EDITION
    57. Comina, PJ; Philp, D; Kariuki, BM; Harris, KDM
      Covalent self-assembly of a dimeric borazaaromatic macrocycle

      CHEMICAL COMMUNICATIONS
    58. Kowalik, JT; Lipinska, T; Oleksyn, BJ; Sliwinski, J
      Conformation of epicinchonine and cinchonine in view of their antimalarialactivity: X-ray and theoretical studies

      ENANTIOMER
    59. Bartok, M; Felfoldi, K; Szollosi, G; Bartok, T
      Rigid cinchona conformers in enantioselective catalytic reactions: new cinchona-modified platinum catalysts in the Orito reaction

      CATALYSIS LETTERS
    60. Bartok, M; Bartok, T; Szollosi, G; Felfoldi, K
      Electrospray ionization mass spectrometry in the heterogeneous catalyzed organic reactions: unknown compounds in the pyruvate hydrogenation

      CATALYSIS LETTERS
    61. Karle, JM; Bhattacharjee, AK
      Stereoelectronic features of the cinchona alkaloids determine their differential antimalarial activity

      BIOORGANIC & MEDICINAL CHEMISTRY
    62. Belokon', YN; Kochetkov, KA; Churkina, TD; Ikonnikov, NS; Vyskocil, S; Kagan, HB
      Enantiomerically enriched (R)- and (S)-alpha-methylphenylalanine via asymmetric PTC C-alkylation catalysed by NOBIN

      TETRAHEDRON-ASYMMETRY
    63. Piette, V; Lammerhofer, M; Lindner, W; Crommen, J
      Enantiomeric separation of N-protected amino acids by non-aqueous capillary electrophoresis using quinine or tert-butyl carbamoylated quinine as chiral additive

      CHIRALITY
    64. Maier, NM; Nicoletti, L; Lammerhofer, M; Lindner, W
      Enantioselective anion exchangers based on cinchona alkaloid-derived carbamates: Influence of C-8/C-9 stereochemistry on chiral recognition

      CHIRALITY
    65. Petri, A; Pini, D; Rapaccini, S; Salvadori, P
      Catalytic asymmetric dihydroxylation of alkenes induced by polymeric chiral ligands

      CHIRALITY
    66. Verma, R; Mithran, S; Ghosh, SK
      Desymmetrization of prochiral anhydrides with Evans' oxazolidinones: an efficient route to homochiral glutaric and adipic acid derivatives

      JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
    67. Leonard, J
      Recent progress in the chemistry of monoterpenoid indole alkaloids derivedfrom secologanin

      NATURAL PRODUCT REPORTS
    68. Bartok, M; Felfoldi, K; Szollosi, G; Bartok, T
      Heterogeneous asymmetric reactions, 14. Epicinchona alkaloids in the enantioselective hydrogenation of ethyl, pyruvate over Pt/alumina. What determines the sense of enantioselection?

      REACTION KINETICS AND CATALYSIS LETTERS
    69. Lygo, B; Crosby, J; Peterson, JA
      Enantioselective alkylation of alanine-derived imines using quaternary ammonium catalysts.

      TETRAHEDRON LETTERS
    70. Belokon, YN; North, M; Kublitski, VS; Ikonnikov, NS; Krasik, PE; Maleev, VI
      Chiral salen-metal complexes as novel catalysts for asymmetric phase transfer alkylations

      TETRAHEDRON LETTERS
    71. Lygo, B; Crosby, J; Lowdon, T; Wainwright, PG
      Asymmetric approaches to 2-hydroxymethylquinuclidine derivatives

      TETRAHEDRON
    72. Zuo, XB; Liu, HF; Guo, DW; Yang, XZ
      Enantioselective hydrogenation of pyruvates over polymer-stabilized and supported platinum nanoclusters

      TETRAHEDRON
    73. Lygo, B; Wainwright, PG
      Phase-transfer catalysed asymmetric epoxidation of enones using N-anthracenylmethyl-substituted cinchona alkaloids

      TETRAHEDRON
    74. Barennes, H
      Unnecessary intramuscular injections in children in subsaharian Africa. A little known pathology: Insuing complications from intramuscular quinine injections.

      BULLETIN DE LA SOCIETE DE PATHOLOGIE EXOTIQUE
    75. Brasic, JR
      Should people with nocturnal leg cramps drink tonic water and bitter lemon?

      PSYCHOLOGICAL REPORTS
    76. Hofstetter, C; Wilkinson, PS; Pochapsky, TC
      NMR structure determination of ion pairs derived from quinine: A model fortemplating in asymmetric phase-transfer reductions by BH4- with implications for rational design of phase-transfer catalysts

      JOURNAL OF ORGANIC CHEMISTRY
    77. Kobayashi, S; Endo, M; Nagayama, S
      Catalytic asymmetric dihydroxylation of olefins using a recoverable and reusable polymer-supported osmium catalyst

      JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
    78. Ooi, T; Kameda, M; Maruoka, K
      Molecular design of a C-2-symmetric chiral phase-transfer catalyst for practical asymmetric synthesis of alpha-amino acids

      JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
    79. Mandl, A; Nicoletti, L; Lammerhofer, M; Lindner, W
      Quinine versus carbamoylated quinine-based chiral anion exchangers - A comparison regarding enantioselectivity for N-protected amino acids and other chiral acids

      JOURNAL OF CHROMATOGRAPHY A
    80. Langer, P; Hoffmann, HMR; Wartchow, R
      Crystal structure of (3S,8R,9R)-3,9-dihydroxy-6 '-methoxy-3-phenyl-10,11-dinorcinchonane hemihydrate, (C24H26N2O3)center dot 0.5H(2)O

      ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES
    81. WELLS PB; WILKINSON AG
      PLATINUM-GROUP METALS AS HETEROGENEOUS ENANTIOSELECTIVE CATALYSTS

      Topics in catalysis
    82. HUTCHINGS GJ; WILLOCK DJ
      HETEROGENEOUS ENANTIOSELECTIVE CATALYSTS - CAN MOLECULAR SIMULATION TECHNIQUES AID THE DESIGN OF IMPROVED CATALYSTS

      Topics in catalysis
    83. SCHRAKE O; BRAJE W; HOFFMANN HMR; WARTCHOW R
      SYNTHESIS OF 10,11-DIDEHYDRO-QUINCORINE AND 10,11-DIHYDRO-QUINCORINE AND OF THE QUINCORIDINE ANALOGS - FUNCTIONALIZED AND ENANTIOPURE 1-AZABICYCLO[2.2.2]-OCTANES WITH 4 STEREOGENIC CENTERS

      Tetrahedron : asymmetry
    84. HEIKKINEN S; MESILAAKSO M; RAHKAMAA E
      NMR SPECTRAL-ANALYSIS AND MOLECULAR-DYNAMICS STUDY OF 3-QUINUCLIDINOLAND 3-QUINUCLIDINYL BENZILATE

      Magnetic resonance in chemistry
    85. Sakai, T; Hirose, A; Sasaki, H
      Extraction spectrophotometric determination of quaternary ammonium salts utilizing ternary ion associate formation with cinchona-alkaloids and tetraiodofluorescein

      BUNSEKI KAGAKU
    86. LANGER P; FRACKENPOHL J; HOFFMANN HMR
      SYNTHESIS OF TRICYCLIC N,O-ACETALS FROM ALPHA-FUNCTIONALIZED RUBANONE- A MASKED 1,2,3-TRICARBONYL SYSTEM FROM QUINIDINE

      Journal of the Chemical Society. Perkin transactions. I
    87. JAESCHKE G; SEEBACH D
      HIGHLY ENANTIOSELECTIVE RING-OPENING OF CYCLIC MESO-ANHYDRIDES TO ISOPROPYL HEMIESTERS WITH TI-TADDOLATES - AN ALTERNATIVE TO HYDROLYTIC ENZYMES

      Journal of organic chemistry
    88. THIEL J; FIEDOROW P
      THE STRUCTURE OF INTERMEDIATE PRODUCTS OF FRAGMENTATION OF 10-BROMODIHYDROCINCHONINE

      Journal of molecular structure
    89. SLIPSZENKO JA; GRIFFITHS SP; JOHNSTON P; SIMONS KE; VERMEER WAH; WELLS PB
      ENANTIOSELECTIVE HYDROGENATION - V - HYDROGENATION OF BUTANE-2,3-DIONE AND OF 3-HYDROXYBUTAN-2-ONE CATALYZED BY CINCHONA-MODIFIED PLATINUM

      Journal of catalysis (Print)
    90. PERTICI P; BORGHERINI F; VITULLI G; SALVADORI P; ROSINI C; MOISE C; BESANCON J
      HIGH-PRESSURE LIQUID-CHROMATOGRAPHY RESOLUTION OF RACEMIC MIXTURES OFCHIRAL TRICARBONYL ARENE CHROMIUM(0) AND CYCLOPENTADIENYL-TITANIUM(IV) COMPLEXES

      Inorganica Chimica Acta
    91. SILVA THA; OLIVEIRA AB; DEALMEIDA WB
      CONFORMATIONAL-ANALYSIS OF THE ANTIMALARIAL AGENT QUININE

      Structural chemistry
    92. PFALTZ A; HEINZ T
      ENANTIOSELECTIVE HYDROGENATION OF ETHYL PYRUVATE OVER PT ALUMINA - SYSTEMATIC VARIATION OF THE MODIFIER STRUCTURE/

      Topics in catalysis
    93. KOHLER JU; BRADLEY JS
      ENANTIOSELECTIVE HYDROGENATION OF ETHYL PYRUVATE WITH COLLOIDAL PLATINUM CATALYSTS - THE EFFECT OF ACIDITY ON RATE

      Catalysis letters
    94. BONNEMANN H; BRAUN GA
      ENANTIOSELECTIVITY CONTROL WITH METAL COLLOIDS AS CATALYSTS

      Chemistry
    95. AKADA Y; KUROGI M
      DETERMINATION OF CINCHONA ALKALOIDS IN CI NCHONA BARK BY CAPILLARY ELECTROPHORESIS

      Bunseki Kagaku
    96. PIETERS RJ; CUNTZE J; BONNET M; DIEDERICH F
      ENANTIOSELECTIVE RECOGNITION WITH C-3-SYMMETRICAL CAGE-LIKE RECEPTORSIN SOLUTION AND ON A STATIONARY-PHASE

      Perkin transactions. 2
    97. SAXTON JE
      RECENT PROGRESS IN THE CHEMISTRY OF THE MONOTERPENOID INDOLE ALKALOIDS

      Natural product reports
    98. LYGO B; CROSBY J; LOWDON TR; WAINWRIGHT PG
      ENANTIOSELECTIVE AND DIASTEREOSELECTIVE SYNTHESIS OF ALL 4 POSSIBLE STEREOISOMERS OF 2-(PHENYLHYDROXYMETHYL)QUINUCLIDINE

      Tetrahedron letters
    99. SCHURCH M; SCHWALM O; MALLAT T; WEBER J; BAIKER A
      ENANTIOSELECTIVE HYDROGENATION OF KETOPANTOLACTONE

      Journal of catalysis
    100. CUNTZE J; DIEDERICH F
      MOLECULAR RECOGNITION AND ENANTIOMER SEPARATIONS ON A NOVEL CHIRAL STATIONARY-PHASE BASED ON A 9,9'-SPIROBI[9H-FLUORENE]-DERIVED MOLECULAR CLEFT

      Helvetica Chimica Acta


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Documento generato il 08/08/20 alle ore 08:28:32