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Titolo:
Electrolytic partial fluorination of organic compounds. Part 48: Anodic fluorination of 2-cyano-1-methylpyrrole
Autore:
Tajima, T; Ishii, H; Fuchigami, T;
Indirizzi:
Tokyo Inst Technol, Dept Elect Chem, Midori Ku, Yokohama, Kanagawa 2268502, Japan Tokyo Inst Technol Yokohama Kanagawa Japan 2268502 anagawa 2268502, Japan
Titolo Testata:
TETRAHEDRON LETTERS
fascicolo: 29, volume: 42, anno: 2001,
pagine: 4857 - 4860
SICI:
0040-4039(20010716)42:29<4857:EPFOOC>2.0.ZU;2-X
Fonte:
ISI
Lingua:
ENG
Soggetto:
5-MEMBERED HETEROAROMATIC-COMPOUNDS; MONOFLUORINATION; SULFIDES; OXIDATION;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Life Sciences
Physical, Chemical & Earth Sciences
Citazioni:
19
Recensione:
Indirizzi per estratti:
Indirizzo: Fuchigami, T Tokyo Inst Technol, Dept Elect Chem, Midori Ku, Nagatsuta, Yokohama, Kanagawa 2268502, Japan Tokyo Inst Technol Nagatsuta Yokohama Kanagawa Japan 2268502
Citazione:
T. Tajima et al., "Electrolytic partial fluorination of organic compounds. Part 48: Anodic fluorination of 2-cyano-1-methylpyrrole", TETRAHEDR L, 42(29), 2001, pp. 4857-4860

Abstract

Anodic fluorination of 2-cyano-1 -methylpyrrole using Et3N . 2HF in an undivided cell provided the corresponding 5-fluoropyrrole and 2,5,5-trifluolo-1-methyl-3-pyrrolin-2-carbonitrile while the use of Et3N . 3HF afforded selectively the latter product, which was readily hydrolyzed to isolable 5,5-difluoro-1-methyl-3-pyrroline-2-one. This is the first report of successful anodic fluorination of a pyrrole derivative. (C) 2001 Elsevier Science Ltd. All rights reserved.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 04/07/20 alle ore 17:35:25