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Titolo:
Liquid chromatographic analysis of streptomycin sulfate
Autore:
Adams, E; Rafiee, M; Roets, E; Hoogmartens, J;
Indirizzi:
Katholieke Univ Leuven, Fac Farmaceut Wetenschappen, Lab Farmaceut Chem & Anal Geneesmiddelen, B-3000 Louvain, Belgium Katholieke Univ Leuven Louvain Belgium B-3000 n, B-3000 Louvain, Belgium
Titolo Testata:
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS
fascicolo: 2, volume: 24, anno: 2000,
pagine: 219 - 226
SICI:
0731-7085(200012)24:2<219:LCAOSS>2.0.ZU;2-Z
Fonte:
ISI
Lingua:
ENG
Soggetto:
PULSED ELECTROCHEMICAL DETECTION; AMPEROMETRIC DETECTION; DIHYDROSTREPTOMYCIN;
Keywords:
streptomycin; liquid chromatography; ultraviolet detection;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Life Sciences
Citazioni:
18
Recensione:
Indirizzi per estratti:
Indirizzo: Roets, E Katholieke Univ Leuven, Fac Farmaceut Wetenschappen, Lab Farmaceut Chem & Anal Geneesmiddelen, E Van Evenstr 4, B-3000 Louvain, Belgium Katholieke Univ Leuven E Van Evenstr 4 Louvain Belgium B-3000 um
Citazione:
E. Adams et al., "Liquid chromatographic analysis of streptomycin sulfate", J PHARM B, 24(2), 2000, pp. 219-226

Abstract

The analysis of streptomycin sulfate using a column packed with base deactivated reversed phase silica gel and ultraviolet (UV) detection at 205 nm is described. The mobile phase consists of an aqueous solution containing 14g/l of sodium sulfate, 1.5 g/l of sodium octanesulfonate. 50 ml/l of acetonitrile and 50 ml/l of a 0.2 M phosphate buffer at pH 3.0. The method allows separating streptidine, streptomycin B. streptomycin and dihydrostreptomycin. as well as several other components. which were not yet identified. The total time of analysis is 50 min. The effects of the different chromatographic parameters on the separation were investigated. A number of commercial samples were analyzed using this method. (C) 2000 Elsevier Science B.V. All rights reserved.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 19/01/20 alle ore 20:51:29