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Titolo:
Synthesis and structural characterization of palladium(II) complex with (L)-3-acetyl-5-benzyl-1-phenyl-4,5-dihydro-1,2,4-triazin-6-one oxime. Part II
Autore:
Abushamleh, AS; El-Abadelah, MM; Mossmer, CM;
Indirizzi:
Univ Jordan, Fac Sci, Dept Chem, Amman, Jordan Univ Jordan Amman JordanUniv Jordan, Fac Sci, Dept Chem, Amman, Jordan Hashemite Univ, Fac Arts & Sci, Dept Chem, Zarka, Jordan Hashemite Univ Zarka Jordan v, Fac Arts & Sci, Dept Chem, Zarka, Jordan Univ Tubingen, Inst Anorgan Chem, D-72076 Tubingen, Germany Univ TubingenTubingen Germany D-72076 n Chem, D-72076 Tubingen, Germany
Titolo Testata:
HETEROCYCLES
fascicolo: 8, volume: 53, anno: 2000,
pagine: 1737 -
SICI:
0385-5414(20000801)53:8<1737:SASCOP>2.0.ZU;2-Y
Fonte:
ISI
Lingua:
ENG
Soggetto:
HETEROCYCLES;
Keywords:
3-acetyl-5-benzyl oxime; bis-oximato Pd(II) complex; X-ray crystal structure;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Physical, Chemical & Earth Sciences
Citazioni:
11
Recensione:
Indirizzi per estratti:
Indirizzo: El-Abadelah, MM Univ Jordan, Fac Sci, Dept Chem, Amman, Jordan Univ Jordan Amman Jordan Sci, Dept Chem, Amman, Jordan
Citazione:
A.S. Abushamleh et al., "Synthesis and structural characterization of palladium(II) complex with (L)-3-acetyl-5-benzyl-1-phenyl-4,5-dihydro-1,2,4-triazin-6-one oxime. Part II", HETEROCYCLE, 53(8), 2000, pp. 1737

Abstract

The synthesis and structural properties of the four-coordinate Pd(L)(2) (4), where L is chiral 3-acetyl-5-benzyl-1-phenyl-4,5-dihydro-1,2,4-triazin-6-one oxime (2), are described. Deep-red needles of 4 crystallize in the hexagonal space group P6(1). The crystallographic data reveal that the two oxime ligands are not symmetrically coordinated to Pd(II) ion, and the 4N-donor set comprises both oxime nitrogens, an amidrazone nitrogen and a hydrazone nitrogen. H-1-, C-13-NMR and FD-MS spectral data of 4 are consistent withits X-Ray molecular structure.

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Documento generato il 21/09/20 alle ore 16:00:17