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Titolo:
Derivatization for electrospray ionization-mass spectrometry. 4. Alkenes and alkynes
Autore:
Van Berkel, GJ; Quirke, JME; Adams, CL;
Indirizzi:
Oak Ridge Natl Lab, Chem & Analyt Sci Div, Oak Ridge, TN 37831 USA Oak Ridge Natl Lab Oak Ridge TN USA 37831 ci Div, Oak Ridge, TN 37831 USA Florida Int Univ, Dept Chem, Miami, FL 33199 USA Florida Int Univ Miami FL USA 33199 Univ, Dept Chem, Miami, FL 33199 USA
Titolo Testata:
RAPID COMMUNICATIONS IN MASS SPECTROMETRY
fascicolo: 10, volume: 14, anno: 2000,
pagine: 849 - 858
SICI:
0951-4198(2000)14:10<849:DFEIS4>2.0.ZU;2-5
Fonte:
ISI
Lingua:
ENG
Soggetto:
ION TRAP; 4-AMINONAPHTHALENESULPHONIC ACID; CHEMICAL DERIVATIZATION; FULLERENE ANIONS; OLIGOSACCHARIDES; METABOLITES; DERIVATIVES; MOLECULES; REAGENT;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Physical, Chemical & Earth Sciences
Citazioni:
44
Recensione:
Indirizzi per estratti:
Indirizzo: Van Berkel, GJ Oak Ridge Natl Lab, Chem & Analyt Sci Div, Oak Ridge, TN 37831 USA Oak Ridge Natl Lab Oak Ridge TN USA 37831 ge, TN 37831 USA
Citazione:
G.J. Van Berkel et al., "Derivatization for electrospray ionization-mass spectrometry. 4. Alkenes and alkynes", RAP C MASS, 14(10), 2000, pp. 849-858

Abstract

A survey of derivatization strategies and prospective derivatization reactions for conversion of simple alkenes and alkynes to 'electrospray-active 'species is presented. General synthetic strategies are discussed and illustrative examples of prospective derivatives prepared from model compounds are presented along with their electrospray ionization (ES) mass spectra, The identified derivatives of these neutral, nonpolar analytes are either ionic or are ionizable in solution through Bronsted acid/base chemistry, by Lewis acid/base chemistry, or by chemical or electrochemical electron-transfer chemistry. Once ionized, the derivatives are expected to be amenable to detection by electrospray ionization-mass spectrometry. Derivatives are identified for positive and negative ion analysis of both alkenes and alkynes. Copyright (C) 2000 John Wiley & Sons, Ltd.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 01/10/20 alle ore 07:02:53