Catalogo Articoli (Spogli Riviste)

OPAC HELP

Titolo:
Analysis of amphetamines by supercritical fluid chromatography, high-performance liquid chromatography, gas chromatography and capillary zone electrophoresis; a preliminary comparison
Autore:
McAvoy, Y; Cole, MD; Gueniat, O;
Indirizzi:
Univ Strathclyde, Dept Pure & Appl Chem, Forens Sci Unit, Glasgow G1 1XW, Lanark, Scotland Univ Strathclyde Glasgow Lanark Scotland G1 1XW G1 1XW, Lanark, Scotland Univ Lausanne, Inst Police Sci & Criminol, CH-1002 Lausanne, Switzerland Univ Lausanne Lausanne Switzerland CH-1002 CH-1002 Lausanne, Switzerland
Titolo Testata:
FORENSIC SCIENCE INTERNATIONAL
fascicolo: 1, volume: 102, anno: 1999,
pagine: 13 - 22
SICI:
0379-0738(19990531)102:1<13:AOABSF>2.0.ZU;2-Q
Fonte:
ISI
Lingua:
ENG
Soggetto:
DRUG SEIZURES; ANALOGS; MS;
Keywords:
amphetamine; methamphetamine; 3,4-methylenedioxyamphetamine (MDA); 3,4-methylenedioxymethylamphetamine; (MDMA, Ecstasy); 3,4-methylenedioxyethylamphetamine (MDEA); supercritical fluid chromatography; high-performance liquid chromatography; gas chromatography; capillary zone electrophoresis;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Clinical Medicine
Citazioni:
15
Recensione:
Indirizzi per estratti:
Indirizzo: Cole, MD Univ Strathclyde, Dept Pure & Appl Chem, Forens Sci Unit, 204 George St, Glasgow G1 1XW, Lanark, Scotland Univ Strathclyde 204 George St Glasgow Lanark Scotland G1 1XW and
Citazione:
Y. McAvoy et al., "Analysis of amphetamines by supercritical fluid chromatography, high-performance liquid chromatography, gas chromatography and capillary zone electrophoresis; a preliminary comparison", FOREN SCI I, 102(1), 1999, pp. 13-22

Abstract

A supercritical fluid chromatographic method with UV detection (SFC-UV) for the quantitative separation of phenylisothiocyanate (PITC)-derivatised amphetamines is described and compared to high-performance liquid chromatography-diode array detection (HPLC-DAD), gas chromatography-flame ionisation detection (GC-FID) and capillary zone electrophoresis-diode array detection (CZE-DAD) analyses of amphetamine and related compounds. Difficulties in the analysis of common amphetamines by SFC are discussed. Of the methods described in this paper, the SFC method offered the greatest sensitivity at 0.01-0.02 mu g of drug on column. Suggestions are made for the use of combinations of these techniques for the identification of amphetamines when gas chromatography-mass spectrometry is not available. (C) 1999 Elsevier Science Ireland Ltd. All rights reserved.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 28/03/20 alle ore 10:15:02