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Titolo:
Validation of the high performance liquid chromatography separation of GLFand related di- and tripeptides
Autore:
Rabouan, S; Prognon, P; Barthes, D;
Indirizzi:
UFR Med & Pharm, Chim Analyt Lab, F-86005 Poitiers, France UFR Med & Pharm Poitiers France F-86005 yt Lab, F-86005 Poitiers, France Facbry, Pharmaceut & Biol Paris Sud, Chim Analyt Lab, F-92290 Chatenay Mala Fac SCi Pharmaceut & Biol Paris Sud Chatenay Malabry France F-92290 Mala
Titolo Testata:
FARMACO
fascicolo: 12, volume: 53, anno: 1998,
pagine: 747 - 751
SICI:
0014-827X(199812)53:12<747:VOTHPL>2.0.ZU;2-E
Fonte:
ISI
Lingua:
ENG
Soggetto:
MILK-PROTEINS; PEPTIDES; COPPER(II); BEHAVIOR;
Keywords:
oligopeptides; high-performance liquid chromatography; glycyl-leucyl-phenylalanine; validation;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Life Sciences
Citazioni:
19
Recensione:
Indirizzi per estratti:
Indirizzo: Barthes, D UFR Med & Pharm, Chim Analyt Lab, BP 199, F-86005 Poitiers, France UFR Med & Pharm BP 199 Poitiers France F-86005 oitiers, France
Citazione:
S. Rabouan et al., "Validation of the high performance liquid chromatography separation of GLFand related di- and tripeptides", FARMACO, 53(12), 1998, pp. 747-751

Abstract

This paper describes a simple and rapid procedure for the determination ofthe important tripeptide glycyl-leucyl-phenylalanine (GLF) and its homologues by reversed phase high-performance liquid chromatography. The eluent for convenient separation on a phenyl-bonded silica stationary phase was 15/85 (v/v) acetonitrile/0.1 M sodium citrate buffer pH 3.0, UV detection was set at 258 nm. The method is specific? linear, accurate (recovery mean = 99.6 +/- 0.8%), and reliable (precision = 1.2%). Limit of detection is established for 0.05 mM and limit of quantification for 0.10 mM (precision = 1.5%). (C) 1998 Elsevier Science S.A. All rights reserved.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 06/04/20 alle ore 21:47:25