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Titolo:
A HIGHLY SENSITIVE METHOD TO IDENTIFY THE D,L-CONFIGURATIONS OF MONOSACCHARIDES BASED ON (-)-TBMB CARBOXYLIC-ACID AND HPLC
Autore:
NISHIDA Y; BAI C; OHRUI H; MEGURO H;
Indirizzi:
TOHOKU UNIV,FAC AGR,DEPT APPL BIOL CHEM,TSUTSUMIDOHRI AMAMIYAMACHI 1-1 SENDAI 981 JAPAN
Titolo Testata:
Journal of carbohydrate chemistry
fascicolo: 7, volume: 13, anno: 1994,
pagine: 1003 - 1008
SICI:
0732-8303(1994)13:7<1003:AHSMTI>2.0.ZU;2-Y
Fonte:
ISI
Lingua:
ENG
Soggetto:
ABSOLUTE-CONFIGURATION; ALCOHOLS; SUGARS;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Science Citation Index Expanded
Science Citation Index Expanded
Citazioni:
11
Recensione:
Indirizzi per estratti:
Citazione:
Y. Nishida et al., "A HIGHLY SENSITIVE METHOD TO IDENTIFY THE D,L-CONFIGURATIONS OF MONOSACCHARIDES BASED ON (-)-TBMB CARBOXYLIC-ACID AND HPLC", Journal of carbohydrate chemistry, 13(7), 1994, pp. 1003-1008

Abstract

D,L-Isomers of monosaccharides were coupled with a fluorescent chiralderivatizing agent, -tert-butyl-2-methyl-1,3-benzodioxole-4-carboxylic acid [(-)-TBMB carboxylic acid], to afford a pair of diastereoisomers. The two were well separated with HPLC (reverse phase conditions; ODS, CH3CN:H2O:isoPrOH) within 60 min and could be detected by fluorescence of the TBMB group at the few picomolar level.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 02/12/20 alle ore 14:29:44