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Titolo:
SYNTHESIS AND X-RAY-ANALYSIS OF 1-((1S)-PHENYLETHYL)-AZETIDINE-(2R)-PIPERIDINAMIDE
Autore:
DEGELDER R; SMITS JMM; STARMANS WAJ; THIJS L; ZWANENBURG B;
Indirizzi:
CATHOLIC UNIV NIJMEGEN,NIJMEGEN SON RES CTR,DEPT INORGAN CHEM,TOERNOOIVELD NL-6525 ED NIJMEGEN NETHERLANDS CATHOLIC UNIV NIJMEGEN,NIJMEGEN SON RES CTR,DEPT ORGAN CHEM NL-6525 ED NIJMEGEN NETHERLANDS
Titolo Testata:
Journal of chemical crystallography
fascicolo: 9, volume: 26, anno: 1996,
pagine: 639 - 642
SICI:
1074-1542(1996)26:9<639:SAXO1>2.0.ZU;2-H
Fonte:
ISI
Lingua:
ENG
Keywords:
CRYSTAL STRUCTURE; CHIRAL AUXILIARIES;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Science Citation Index Expanded
Science Citation Index Expanded
Citazioni:
13
Recensione:
Indirizzi per estratti:
Citazione:
R. Degelder et al., "SYNTHESIS AND X-RAY-ANALYSIS OF 1-((1S)-PHENYLETHYL)-AZETIDINE-(2R)-PIPERIDINAMIDE", Journal of chemical crystallography, 26(9), 1996, pp. 639-642

Abstract

The crystal and molecular structure of a new azetidine-2-carboxylic amide derivative is described. The structure was solved by direct methods and refined by least squares methods to R1 = 0.0393 for 4264 reflections (with I > 2 sigma(I)). The structure consists of two independentmolecules which are chemically the same with slight differences in geometry. Crystal data: C17H24N2O, monoclinic, space group P2(1), a = 8.3782(4), b = 20.0342(13), c = 9.7769(8)Angstrom, beta = 109.687(6)degrees, V = 1545.1(2)Angstrom(3), Z = 4.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 27/11/20 alle ore 10:45:31