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Titolo:
A HIGHLY SENSITIVE HPLC METHOD TO DISCRIMINATE ENANTIOMERIC AMINO DEOXY SUGARS BASED ON THE DERIVATIZATION WITH (S)-(-TBMB CARBOXYLIC-ACID())
Autore:
BAI C; NISHIDA Y; OHRUI H; MEGURO H;
Indirizzi:
TOHOKU UNIV,FAC AGR,DEPT APPL BIOL CHEM,AMAMIYAMACHI 1-1 SENDAI MIYAGI 981 JAPAN
Titolo Testata:
Journal of carbohydrate chemistry
fascicolo: 2, volume: 15, anno: 1996,
pagine: 217 - 230
SICI:
0732-8303(1996)15:2<217:AHSHMT>2.0.ZU;2-C
Fonte:
ISI
Lingua:
ENG
Soggetto:
GALACTOSYLTRANSFERASE;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Science Citation Index Expanded
Science Citation Index Expanded
Citazioni:
16
Recensione:
Indirizzi per estratti:
Citazione:
C. Bai et al., "A HIGHLY SENSITIVE HPLC METHOD TO DISCRIMINATE ENANTIOMERIC AMINO DEOXY SUGARS BASED ON THE DERIVATIZATION WITH (S)-(-TBMB CARBOXYLIC-ACID())", Journal of carbohydrate chemistry, 15(2), 1996, pp. 217-230

Abstract

A picomole determination of the absolute configurations of amino deoxy sugars was demonstrated through the derivatization at the anomeric carbon with a fluorescent chiral reagent, (S)-(+)-TBMB carboxylic acid,followed by the HPLC separations of the derived diastereomeric isomers. Anew chemical procedure was developed to convert amino deoxy sugarsinto per-NH,O-acetylated glycosyl chlorides prior to derivatization with the reagent.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 24/11/20 alle ore 10:54:06