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Titolo:
DETERMINATION OF THE ABSOLUTE-CONFIGURATIONS AND TOTAL SYNTHESIS OF NEW IMMUNOSUPPRESSANTS, MYCESTERICIN-E AND MYCESTERICIN-G
Autore:
FUJITA T; HAMAMICHI N; MATSUZAKI T; KITAO Y; KIUCHI M; NODE M; HIROSE R;
Indirizzi:
SETSUNAN UNIV,FAC PHARMACEUT SCI,45-1 NAGAOTOGE CHO HIRAKATA OSAKA 57301 JAPAN KYOTO PHARMACEUT UNIV,YAMASHINA KU KYOTO 607 JAPAN KYOTO UNIV,FAC PHARMACEUT SCI,SAKYO KU KYOTO 60601 JAPAN TAITO CO LTD,RES LAB,NAGATA KU KOBE HYOGO 653 JAPAN
Titolo Testata:
Tetrahedron letters
fascicolo: 47, volume: 36, anno: 1995,
pagine: 8599 - 8602
SICI:
0040-4039(1995)36:47<8599:DOTAAT>2.0.ZU;2-1
Fonte:
ISI
Lingua:
ENG
Soggetto:
DERIVATIVES;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Science Citation Index Expanded
Citazioni:
11
Recensione:
Indirizzi per estratti:
Citazione:
T. Fujita et al., "DETERMINATION OF THE ABSOLUTE-CONFIGURATIONS AND TOTAL SYNTHESIS OF NEW IMMUNOSUPPRESSANTS, MYCESTERICIN-E AND MYCESTERICIN-G", Tetrahedron letters, 36(47), 1995, pp. 8599-8602

Abstract

The absolute configurations of two new immunosuppressants, mycestericins E (1) and G (2), were established and both compounds were synthesized starting from 1,8-octanediol and a fully protected methyl (2S,4R)-oxazolidine-4-carboxylate 3. Compounds 5 and 22, with a(1'R)-hydroxyl group, were prepared from the beta-keto esters 4 and 21, respectively,by stereoselective reduction with metal borohydrides.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 09/07/20 alle ore 13:45:18