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Titolo:
Neutral mononuclear and binuclear hexacoordinate silicon complexes with SiO5C skeletons
Autore:
Tacke, R; Burschka, C; Willeke, M; Willeke, R;
Indirizzi:
Univ Wurzburg, Inst Anorgan Chem, D-97074 Wurzburg, Germany Univ WurzburgWurzburg Germany D-97074 n Chem, D-97074 Wurzburg, Germany
Titolo Testata:
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
fascicolo: 7, , anno: 2001,
pagine: 1671 - 1674
SICI:
1434-1948(200107):7<1671:NMABHS>2.0.ZU;2-L
Fonte:
ISI
Lingua:
ENG
Soggetto:
PENTACOORDINATE; STEREOCHEMISTRY; REACTIVITY;
Keywords:
chelates; coordination chemistry; silicates; macrocycles; silicon;
Tipo documento:
Article
Natura:
Periodico
Settore Disciplinare:
Physical, Chemical & Earth Sciences
Citazioni:
14
Recensione:
Indirizzi per estratti:
Indirizzo: Tacke, R Univ Wurzburg, Inst Anorgan Chem, Hubland, D-97074 Wurzburg, Germany Univ Wurzburg Hubland Wurzburg Germany D-97074 Wurzburg, Germany
Citazione:
R. Tacke et al., "Neutral mononuclear and binuclear hexacoordinate silicon complexes with SiO5C skeletons", EUR J INORG, (7), 2001, pp. 1671-1674

Abstract

Treatment sf the silanes (EtO)(3)Si(CH2)(2)SCH2C(O)OSiMe3 and (EtO)(3)Si(CH2)(3)OSiMe3 with two molar equivalents of 1-hydroxy-2-pyridone in acetonitrile yielded the neutral hexacoordinate silicon complexes bis[mu-(3-thiapentanoato(2-)-C-5,O',C5',O)]tetrakis[1-oxopyridin-2-olato(1-)]disilicon(IV) (6) and bis[1-oxopyridin-2-olato(1-)][propanolato(2-)-C-3,O]-silicon(IV) (8), respectively. The compounds 6 . 2CH(3)CN and 8 were characterized by solid-state Si-29 VACP/MAS NMR spectroscopy, mass spectrometry (FAB MS), and single-crystal X-ray diffraction.

ASDD Area Sistemi Dipartimentali e Documentali, Università di Bologna, Catalogo delle riviste ed altri periodici
Documento generato il 18/11/17 alle ore 03:46:19